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CasNo： 461-18-7
MF： C4H7F3O
InChI:InChI=1/C7H4ClF3O/c8-5-1-3-6(4-2-5)12-7(9,10)11/h1-4H
The invention discloses a novel synthesi...
The invention discloses a method for syn...
The invention provides a method for prep...
The present invention provides a novel c...
ethyl 4,4,4-trifluorobutanoate
4,4,4-trifluorobutanol
| Conditions | Yield |
|---|---|
|
ethyl 4,4,4-trifluorobutanoate;
With
sodium tetrahydroborate;
In
tetrahydrofuran;
for 1h;
With
calcium chloride;
In
tetrahydrofuran;
at 70 ℃;
|
86.03% |
|
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 3h;
Heating;
|
53% |
|
With
lithium aluminium tetrahydride; diethyl ether;
|
4,4,4-trifluorobutanal
4,4,4-trifluorobutanol
| Conditions | Yield |
|---|---|
|
With
tetrabutylammonium borohydride;
In
tetrahydrofuran;
at -10 - 20 ℃;
for 3h;
Reagent/catalyst;
Temperature;
Inert atmosphere;
|
83% |
|
With
lithium aluminium tetrahydride; diethyl ether;
|
4,4,4-trifluorobutanal
4,4,4-trifluorobutyric acid
ethyl 4,4,4-trifluorobutanoate
ethyl 4,4,4-trifluorobut-2-enoate
4,4,4-trifluorobutanal
1-Bromo-4,4,4-trifluorobutane
1,1,1-trifluoro-4-iodo-butane
4,4,4-trifluorobutyl 4-methylbenzenesulfonate
